Another thing: MnO2 is the major product of KMnO4 oxidation, and even that can oxidize benzyl alcohol to benzaldehyde. mechanism for the oxidation of benzyl alcohol using nitric acid is proposed, showing the reversible formation of benzyl nitrite and its irreversible decomposition to benzaldehyde… Certified DIY. This method works great and yields are always good - 92% and up. Benzyl alcohol is an easily obtainable chemical, it is a common paint remover. Concerning the benzyl alcohol oxidation to benzaldehyde in the absence of alkali, early reports deal principally with liquid phase reactions which rarely reach the total conversion and show a selectivity in the range of 90–100% in spite of a quite low TOF , , , , . So take that into consideration when calculating stoichiometry. It even scales well (tested with 1.5 liters of Benzyl alcohol in a single run). - Free download as PDF File (.pdf), Text File (.txt) or read online for free. I believe the way I've done it is by having the KMnO4 in an aqueous layer and just stirred vigorously with low heat. Benzyl Alcohol to Benzaldehyde oxidation w/Nitric acid - 92%+ yield.
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